Aspen Technology Aspen Process Manual Contents www.aspentech.com   support.aspentech.com 
Web site | Process Manual > Solids and separation > Solid liquid separation | Word index

SLS 2: Cake Filtration

SLS 2: Cake Filtration
     Volume 2A: Fundamentals and Design
         Part 1: Introduction
             1. INTRODUCTION
                 1.1 Scope and Contents of Volume
         Part 2: Modelling Filtration Processes
             MODELLING FILTRATION PROCESSES
             1 POROSITY, SYMBOL e, DIMENSIONLESS
             2 CAKE SATURATION, SYMBOL S, DIMENSIONLESS
             3 MOISTURE CONTENT, SYMBOL m, DIMENSIONLESS
                 3.1 Conversion between Parameters
             4 CAKE PERMEABILITY (SYMBOL B, UNITS m 2 )
                 4.1 Definition
                 4.2 The Kozeny Equation
                 4.3 Limitations of Kozeny Equation
             5 CAKE RESISTANCE (also known as specific cake resistance)
                 5.1 Cake Compressibility
             6 CLOTH RESISTANCE
                 6.1 Clean Cloth Resistance
                 6.2 Used Cloth Resistance
             7 FILTRATION MECHANISMS
             8 CLARIFICATION
             9 CAKE FORMATION
                 9.1 Incompressible Cakes
                 9.2 Compressible Cakes
                 9.3 Limitations of Cake Formation Equations
             10 METHODS OF DEWATERING
             11 CAKE DEWATERING BY GAS FLOW
                 11.1 Capillary Pressure Curves
                 11.2 Breakthrough Pressure, symbol P b , units Pa
                 11.3 Equilibrium Saturation, Symbol S r , dimensionless
                 11.4 Dewatering Rates
                 11.5 Gas Flowrate
                 11.6 Evaporation Effects in Gas Blowing
             12 CAKE DEWATERING BY COMPRESSION
                 12.1 High Pressure Filtration in Leaf Filters
                 12.2 Filters with Rubber Diaphragms (Compression Filters)
                 12.3 High Pressure Filtration in Filter Presses
                 12.4 Compression by Changes In Flow Direction
                 12.5 Compression on Belt Presses
             13 WASHING
                 13.1 Reslurry Washing
                 13.2 Displacement Washing
         Part 3: Filter Design and Optimisation
             FILTER DESIGN AND OPTIMISATION
             1 DATA COLLECTION
                 1.1 Process Limitations
                 1.2 Properties of Feed Slurry
                 1.3 Required Properties of the Products
             2 SELECTION OF FILTER TYPES
             3 CONTROL OF FILTERS
             4 VARIABLES TO OPTIMISE
             5 CLOTH SELECTION
             6 COLLECTION OF REPRESENTATIVE SAMPLE
             7 OPTIMISATION
                 7.1 Optimisation of Batch Filters
                 7.2 Evaporation in Gas Blowing
                 7.3 Dewatering in a Diaphragm Press
                 7.4 Washing
         Part 4: Testwork
             TESTWORK
             1 EQUIPMENT FOR LABORATORY SCALE TESTWORK
                 1.1 Vacuum Filters
                 1.2 Pressure Leaf Filters
                 1.3 Chamber Filters (e.g. Recessed Plate Filters)
                 1.4 Batch Compression Filters
                 1.5 Belt Presses
                 1.6 Pilot-Scale Testing
             2 PROCEDURES FOR LABORATORY-SCALE TESTING
                 2.1 Flocculation
                 2.2 Precoating
                 2.3 Thickening
                 2.4 Other Pretreatment Methods
                 2.5 Chamber Filling
                 2.6 Cake Formation
                 2.7 Dewatering by Gas Blowing
                 2.8 Washing
                 2.9 Compression
                 2.10 Discharge
         Part 5: Analysis of Data
             ANALYSIS OF DATA
             1 CAKE FORMATION
                 1.1 Cake Properties
                 1.2 Filtrate Flowrate Data
                 1.3 Cake Thickness
                 1.4 Area of Filter Required
                 1.5 t/V vs V Plots with Anomalous Features
                 1.6 Extension of Data
             2 DEWATERING BY GAS FLOW
                 2.1 Pressure Required
                 2.2 Collection of Data
                 2.3 Extension of Data
                 2.4 Gas Flowrates
             3 COMPRESSION
                 3.1 Equilibrium Porosity
                 3.2 Continuous Compression
                 3.3 Compression Rates
                 3.4 Compression in Filter Presses.
             4 WASHING
                 4.1 Reslurry Washing
                 4.2 Displacement Washing
             5 SCOPING DESIGN WHEN SAMPLES NOT AVAILABLE
                 5.1 Cake Formation
                 5.2 Washing
                 5.3 Dewatering by Gas Blowing
                 5.4 Dewatering by Evaporation
         Part 6: Alternative Definitions
             1 DEFINITIONS OF VOIDAGE
             2 ALTERNATIVE EQUATIONS FOR PERMEABILITY
                 2.1 Definitions of Permeability based on Time for Cake Formation.
                 2.2 Alternative Definitions of Cake Resistance
             3 ALTERNATIVE EQUATIONS FOR PERMEABILITY
                 3.1 Permeability as a Function of Size Distribution
             4 ALTERNATIVE EQUATIONS FOR FLOW WHEN INERTIAL EFFECTS ARE SIGNIFICANT
             5 EFFECT OF PRESSURE UPON CAKE RESISTANCE
             6 EFFECT OF PRESSURE ON POROSITY
             7 CONVERSION FACTORS FOR CLEAN CLOTH RESISTANCE
                 7.1 Other Ways of Characterising Cloths
             8 ALTERNATIVE WAYS OF PLOTTING CAKE FORMATION DATA
                 8.1 Constant Pressure Data
                 8.2 Constant Rate Data
             9 CORRELATIONS FOR RESIDUAL SATURATION
             10 ALTERNATIVE EXPRESSIONS FOR DE-WATERING RATES
             11 ALTERNATIVE EXPRESSIONS FOR GAS FLOW DURING DE-WATERING
             12 ALTERNATIVE EQUATIONS FOR DE-WATERING IN FILTER PRESSES
             13 SOLUTION OF DISPERSION EQUATION
         Part 7: Nomenclature
             SYMBOLS
         Part 8: References
             REFERENCES
         Part 9: Dewatering of filter cakes
             0. Preface
             1. Introduction
             2. Methods of filter cake dewatering and their applicability
             3. Dewatering by gas blowing and liquid displacement
             4. Dewatering by gravity and centrifugal drainage
             5. Dewatering by decompression
             6. Nomenclature
             7. References
         Part 10: Washing of cakes and thickened slurries
             0. Preface
             1. Introduction
             2. Basic washing concepts
             3. Obtaining and presenting washing data
             4. Washing calculations
             5. Fundamental models for cake washing
             6. Washing arrangements for solid-liquid separations
             7. The selection of use of wash nozzles and weirs
             8. Selection of a wash liquid
             9. The control of washing systems
             10. Optimisation of the washing stage
             11. Conclusions
             12. Nomenclature
             13. References
         Part 11: The sizing of vacuum filters
             0. Preface
             1. Introduction
             2. Data collection and consideration of options
             3. Testwork
             4. Optimisation
             5. Mechanical design and ancillaries
             6. Nomenclature
             7. References
         Part 12: Dewatering by Gas Blowing
             0. Preface
             1. Introduction
             2. Design methods suitable for quick cost estimations
             3. Design procedure
             4. Discussion of certain aspects of the design procedure
             5. Nomenclature
             6. References
     Volume 2B: Equipment
         Part 1: Introduction
             1. INTRODUCTION
                 1.1 Scope of Volume
                 1.2 Contents of Volume
                 1.3 Glossary
         Part 2: Nutsche Filters
             1. INTRODUCTION
             2. EQUIPMENT
                 2.1 Gravity, vacuum and pressure nutsches
                 2.2 Pressure Nutsches for Integrated Processing
             3. SELECTION
                 3.1 Introduction
                 3.2 Gravity, Vacuum and Pressure Nutsches
                 3.3 Pressure Nutsches for Integrated Processing
             4. OPERATION
                 4.1 Introduction
                 4.2 Gravity, Vacuum and Pressure Nutsches
                 4.3 Pressure Nutsches for Integrated Processing
             5. REFERENCES
         Part 3: Disc and Drum Filters
             1. INTRODUCTION
                 1.1 Scope and Objectives
                 1.2 Glossary
             2. EQUIPMENT
                 2.1 Equipment Options
                 2.2 Disc filters
                 2.3 Bottom fed multi-compartment drums
                 2.4 Bottom fed single compartment drum filters
                 2.5 Internally fed drum filters
                 2.6 Multi-compartment vacuum top fed drums
             3. SELECTION
                 3.1 Introduction
                 3.2 Selection of features appropriate to your feed
                 3.3 Process requirements
                 3.4 Equipment costs
             4. OPERATION
                 4.1 Introduction
                 4.2 Installation and start-up
                 4.3 Control
                 4.4 Filter maintenance
                 4.5 Operating problems and solutions
             5. REFERENCES
         Part 4: Belt Filters
             1. SCOPE AND CONTENTS
                 1.1 Scope of this part
                 1.2 Contents of Part
                 1.3 Glossary
             2. EQUIPMENT OPTIONS
                 2.1 Conveyor belts
                 2.2 Linear screens
                 2.3 Paper forming belts
                 2.4 Low vacuum belts
                 2.5 Belt filters for clarification
                 2.6 Submerged belts
                 2.7 Rubber belt filters
                 2.8 Reciprocating tray filter
                 2.9 Intermittent belt filters with short cycle times
                 2.10 Intermittent filters with long cycle times
                 2.11 Travelling pan filter
                 2.12 Rigid belt filter
             3. SELECTION AND APPLICATIONS
                 3.1 Comparison of belt with other vacuum filters
                 3.2 Selection of type of belt filter
                 3.3 Comparison of belt with pressure filters
             4. INSTALLATION, OPERATION AND MAINTENANCE
                 4.1 Ancillary equipment
                 4.2 Instrumentation and control
                 4.3 Installation of belt filters
                 4.4 Utilities and maintenance
                 4.5 Operating experiences
             5. REFERENCES
         Part 5: Continuous Tipping Pan and Table Filters
             1. INTRODUCTION
             2. EQUIPMENT
                 2.1 Equipment Options
                 2.2 Tipping Pan Filters
                 2.3 Table Filters
             3. SELECTION
             4. OPERATION
                 4.1 Introduction
                 4.2 Installation
                 4.3 Control
                 4.4 Filter Maintenance
                 4.5 Operating Experiences
             5. REFERENCES
         Part 6: Batch Tank Filters
             1. INTRODUCTION
                 1.1 Background and Objectives
                 1.2 Glossary
             2. EQUIPMENT OPTIONS FOR BATCH TANK FILTERS
                 2.1 Overview of Equipment Options
                 2.2 Features of Tank Filters
             3. SELECTION
                 3.1 Selection Procedure
                 3.2 Media Selection
                 3.3 Equipment features
                 3.4 Process Requirements
                 3.5 Feed and product characteristics
                 3.6 Effect of constructional features on capital cost
             4. OPERATION OF BATCH TANK FILTERS
                 4.1 Introduction
                 4.2 Precoating
                 4.3 Filtration
                 4.4 Slurry heel treatment
                 4.5 Cake Washing
                 4.6 Cleaning
                 4.7 Inspection and maintenance
                 4.8 Operating problems and solutions
             5. REFERENCES
         Part 7: Continuous Pressure Filters
             1. INTRODUCTION
             2. EQUIPMENT
                 2.1 Equipment Options
                 2.2 Basic Designs of Continuous Pressure Filters
                 2.3 Specialised Designs
             3. REFERENCES
         Part 8: Filter Presses
             1. INTRODUCTION
                 1.1 Glossary
             2. EQUIPMENT OPTIONS
                 2.1 Introduction
                 2.2 Plate and Frame Presses
                 2.3 Recessed Plate Presses
                 2.4 Vertical Presses (Horizontal Plates)
                 2.5 Plate Support
                 2.6 Plates
                 2.7 Frames
                 2.8 Opening and Closing Mechanism
                 2.9 Filtrate Collection
                 2.10 Plate Separators
                 2.11 Cake Release Devices
                 2.12 Cloth Washing
                 2.13 Automatic Presses
                 2.14 Filter Media
             3. SELECTION
                 3.1 Vertical or Horizontal Plates
                 3.2 Recessed Plates or Plate and Frame
                 3.3 Size and Number of Plates
                 3.4 Side Bar or Overhead Beam Press
                 3.5 Manual, Mechanised, Fully Mechanised or Automatic Press
                 3.6 Position of Ports
                 3.7 Filter Media
                 3.8 Costs
             4. OPERATION
                 4.1 Installation
                 4.2 Medium Fitting
                 4.3 Pumps
                 4.4 Commissioning
                 4.5 Maintenance
                 4.6 Labour
                 4.7 Pretreatment
                 4.8 Precoating
                 4.9 Filtration
                 4.10 Cake Washing
                 4.11 Core Blowing
                 4.12 Gas Blowing
                 4.13 Cake Discharge
                 4.14 Cloth and Plate Washing
                 4.15 Cloth Lifetimes
                 4.16 Control
                 4.17 Problems
             5. REFERENCES
         Part 9: Batch Compression Equipment
             1. INTRODUCTION
             2. EQUIPMENT OPTIONS
                 2.1 Introduction
                 2.2 Commercially-available Equipment
                 2.3 Obsolete Equipment
                 2.4 Summary of Batch Compression Filters
             3. SELECTION
                 3.1 Introduction
                 3.2 The Impact of Higher Pressure
                 3.3 Preliminary Selection
             4. OPERATION: SOME TYPICAL PERFORMANCE DATA
                 4.1 Diaphragm plate filter press
                 4.2 Tower press
                 4.3 Tube press
                 4.4 Bucher 'Universal' press
                 4.5 Generale Sucriere 'Ultrapresse'
                 4.6 Sico-W.A.P. 'Wring Alternating Press'
             5. REFERENCES
                 5.1 Journals and Books cited
                 5.2 Equipment Suppliers
         Part 10: Vacuum Compression Filters
             1. INTRODUCTION
             2. EQUIPMENT OPTIONS
                 2.1 Commercially Available Equipment
                 2.2 OBSOLETE EQUIPMENT
                 2.3 SUMMARY OF CONTINUOUS COMPRESSION DEWATERING EQUIPMENT
             3. SELECTION
                 3.1 Introduction
                 3.2 Physical Form Of Feed Material
                 3.3 Filter Media
                 3.4 Compressive Pressure
                 3.5 Washing Of The Solids
                 3.6 Typical Performance Data
             4. OPERATION: SOME TYPICAL PERFORMANCE DATA
                 4.1 Introduction
                 4.2 Ancillaries For Conventional Vacuum Filters
                 4.3 Drum Type Filters
                 4.4 Disc Type Filters - the Fournier 'Rotary Press'
                 4.5 Horizontal Belt Filters With Compression Stage
                 4.6 Belt Presses (Multi-Roll)
                 4.7 Screw Presses
                 4.8 Ram.Presses
                 4.9 REFERENCES
                 4.10 JOURNALS AND BOOKS CITED
                 4.11 EQUIPMENT SUPPLIERS
         Part 11: Filter Control
             1. SCOPE OF THIS PART
             2. METHODS OF CONTROL
                 2.1 Reasons for Control
                 2.2 Requirements of a Control System
                 2.3 Types of Control
             3. CONTROL OF SPECIFIC OPERATIONS
                 3.1 Flocculation
                 3.2 Precoating
                 3.3 Cake Formation
                 3.4 Washing
                 3.5 Dewatering by Gas Flow
                 3.6 Dewatering by Compression
                 3.7 Filtrate Clarity
             4. CONTROL OF SPECIFIC FILTER TYPES
                 4.1 Batch Filters
                 4.2 Continuous Filters
             5. CHECKLISTS
                 5.1 Measured Variables
                 5.2 Manipulated Variables
                 5.3 Parameters to Keep Constant
                 5.4 Other Factors
             6. REFERENCES
         Part 12: Ancillary Equipment for Cake Filters
             1. HOW TO USE THIS PART
             2. LAYOUT AND SAFETY
                 2.1 Layout
                 2.2 Safety and Loss Prevention
             3. EQUIPMENT ITEMS
                 3.1 Introduction and Flowsheets
                 3.2 Pipes
                 3.3 Valves
                 3.4 Slurry Transfer to Filter
                 3.5 Receivers for Filtrate Collection
                 3.6 Foam Breaking
                 3.7 Filtrate Removal
                 3.8 Vacuum Generation
                 3.9 Treatment of Exhaust Gases
                 3.10 Compressed Gas Supply
                 3.11 Inert Gas Supply and Blanketing
                 3.12 Vents
                 3.13 Precoating and Body Feed Systems
                 3.14 Flocculation
                 3.15 Cake Washing
                 3.16 Media Cleaning
                 3.17 Filter System Cleaning
             4. REFERENCES
         Part 13: Performance Improvement
             1. PROCEDURE FOR IMPROVING FILTER PERFORMANCE
                 1.1 Reasons to improve filter performance
                 1.2 Specify Problem
                 1.3 Generate Possible Solutions
                 1.4 Identify Effects of Proposed Solutions
                 1.5 Quantify Effects of Possible Solutions
                 1.6 Optimising the Solutions
             2. CHECKLISTS OF POSSIBLE SOLUTIONS
                 2.1 Low Throughput
                 2.2 High Moisture Content
                 2.3 Poor Washing
                 2.4 Poor Filtrate Clarity

Volume SLS IIA : Cake Filtration - Fundamentals and Design.

Volume SLS IIA : Part 1 Introduction

This part describes briefly the scope and contents of Volume IIA


Volume SLS IIA : Part 2  Modelling filtration processes

This part contains some basic definitions and simple models which can be used to simulate filtration processes. Only models of practical use to industrialists are included; other models given in the literature are difficult (or impossible) to use in practical situations. The models in this part can be used to estimate filtration characteristics from particle properties and to extend the range of data so minimising the amount of testwork required.


Volume SLS IIA : Part 3  Filter design and optimisation

This part describes the general approach for designing new filters.


Volume SLS IIA : Part 4  Testwork

This part describes simple laboratory scale equipment which can be used to simulate full scale filters, and shows how the tests should be carried out. The laboratory scale equipment includes vacuum filters, pressure leaf filters, chamber filters, batch compression filters and belt presses. Procedures for laboratory-scale testing cover flocculation, precoating, thickening, and other pretreatment methods, as well as chamber filling, cake formation, dewatering by gas blowing, washing, compression and discharge.


Volume SLS IIA : Part 5  Analysis of data

This part shows, with the aid of worked examples, how the data from the testwork should be treated. It also shows how the data can be extended to give an optimum design by using the equations given in Part 2.


Volume SLS IIA : Part 6  Alternative definitions.

This part gives definitions and equations which are alternatives to those given in Part 2. In general, these are equations which are not recommended but which the reader may find in the literature. Where appropriate, the relationship between the recommended and alternative equations are given.


Volume SLS IIA : Part 7  Nomenclature

Volume SLS IIA : Part 8  References


Existing Reports

The reduction in the moisture content of filter cakes. (SAR 6) (Rev)

The methods of dewatering covered are gas blowing including hot gas and steam blowing; gravity and centrifugal drainage; and mechanical compression in batch machines (filter presses, diaphragm presses) and continuous machines (belt presses, screw presses, rolls on vacuum filters). The report is concerned more with the process of dewatering rather than with equipment. For each method, the report describes the mechanisms, the theoretical models and design methods. The report shows how to optimise the performance by manipulating process variables or by flocculating the feed. A selection guide is given to allow the user to decide which method to use.

The washing of cakes and thickened slurries. (SAR 50)

The basic concepts of reslurry and displacement washing are first explained. Then methods are described for carrying out laboratory test work for obtaining washing data. Methods are given for calculating the performance of single and multi-stage co-current and counter-current operations from the test data. Fundamental models for predicting the behaviour of cakes during washing are described. There is a description of the washing arrangements for gravity, vacuum, pressure, compression, centrifugal and membrane filters and for sedimentation equipment, screens and washing columns. The design and selection of spray nozzles, weirs and wash troughs is discussed with particular attention to the problem of applying small amounts of wash liquid. Selection of the wash liquid is discussed in relation to viscosity, density, temperature, polarity, volatility and reactivity. Methods of controlling the volume and temperature of the wash liquid and effluents are described. Optimisation of the washing stage is discussed in relation to drum, belt and leaf filters as is the relation between cake formation, dewatering and washing.

The sizing of vacuum filters. (DR 20)

The report presents in logic diagram form a procedure for sizing filters. The procedure requires that data should be collected on the process limitations, on the properties of the feed stream, and the required properties of the product streams. Decisions can then be made on the type of filter to use and on which variables are available for optimisation. A suitable cloth is selected at this stage. Test work should then be done with a representative sample of slurry and should simulate full-scale conditions as closely as possible. The leaf test is used for most of the test work but the CST test and pilot-scale testing may play some part. Design factors are given for scaling up the results from the leaf test. Methods of optimising the design are given for six different filter applications. The final stage is to consider the mechanical design of the filter and to specify the ancillaries.

Dewatering by gas blowing. (DR 25)

The report describes design methods for dewatering of filter cakes by gas blowing, in the absence of evaporation effects. The methods can be used for vacuum or pressure filters and give rate of desaturation and gas flow required. A quick method is given in which dewatering characteristics are calculated from known cake properties. This method requires no test work but is suitable only for initial costing. The main design method requires a limited amount of test work but correlations are given to extrapolate the data to longer dewatering times and thicker cakes. Design factors are given for scale-up to full size. Details of the test work required are given and the analysis of the results is illustrated with worked examples. Alternative methods of dewatering cakes are discussed and methods of optimising the design given.

 


 

Volume SLS IIB : Cake Filtration - Equipment.

Volume SLS IIB : Part 1 Introduction

This part gives an overview of the volume including sections on the scope and contents. It also gives a glossary of terms used in the volume.


Volume SLS IIB : Part 2 to 10 Nutsches

Parts 2-10 each describe the available equipment options. They show when to use one option in preference to another and give advice on the installation, operation and maintenance of the equipment. Some information on compression filters can be found in Volume IIA.


Volume SLS IIB : Part 11  Control of filters

This part provides a checklist of factors which should be considered when deciding how to control a cake filter. It is illustrated with examples of typical control methods. Different methods of control are reviewed and the requirements of a control system are listed. Typical control variables and manipulated variables are given for various filtration operations. Typical control strategies are given for a number of types of filter.


Volume SLS IIB : Part 12  Ancillary equipment

This part helps the reader to select ancillary equipment for cake filters. It covers safety and layout as well as specific pieces of equipment such as tanks, pumps and valves.


Volume SLS IIB : Part 13  Performance improvement

This part consists of a check list of possible ways of improving filter performance. A computer program based on this Part (CAKEFIMP) is on the CD-ROM.