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DRY 3: Fluidised Bed Drying

DRY 3: Fluidised Bed Drying
     Part 1: Introduction
         1. HOW TO USE THIS MANUAL
         2. BASIC FEATURES OF FLUIDISED BED DRYING
             2.1 Description
             2.2 Underlying processes
             2.3 Comparison with other dryer types
         3 REFERENCES
     Part 2: State of the Technology
         1. INTRODUCTION
         2. BATCH FLUIDISED BEDS
         3. CONTINUOUS FLUIDISED BEDS
             3.1 Introduction
             3.2 Well-mixed fluidised beds
             3.3 Plug-flow fluidised beds
             3.4 Multi-stage fluidised beds
             3.5 Beds with internal heating
             3.6 Vibro-fluidised bed dryers
             3.7 Fluidised bed granulation and coating
             3.8 Fluidised bed coolers
             3.9 Basic design considerations
         4. ANCILLARY EQUIPMENT
             4.1 Gas feed system
                 4.1.1 Selection of fluidising gas
                 4.1.2 Air inlet system
                 4.1.3 Heater system
                 4.1.4 Plenum chamber
                 4.1.5 Distributor plate
             4.2 Solids feeding mechanism
             4.3 Product discharge
             4.4 Freeboard region and gas cleaning systems
             4.5 Materials of construction
         5. OTHER RELATED DRYER TYPES
         6. OPERATING EXPERIENCE
             6.1 Control and instrumentation
             6.2 Startup and shutdown
             6.3 Maintenance
             6.4 Energy utilisation
             6.5 Costs
                 6.5.1 Capital cost
                 6.5.2 Operating cost
         7. SAFETY AND ENVIRONMENTAL CONSIDERATIONS
             7.1 Safety
                 7.1.1 Types of hazard
                 7.1.2 Fire hazards
                 7.1.3 Dust explosions
                 7.1.4 Vapour explosions
             7.2 Environmental considerations
                 7.2.1 Gaseous emissions
                 7.2.2 Odour
                 7.2.3 Particulate emissions
         8. APPLICATIONS
             8.1 Introduction
             8.2 Industrial applications
         9 REFERENCES
     Part 3: State of the Science
         1. INTRODUCTION
         2. FLUIDISATION
             2.1 Introduction
             2.2 The fluidisation process
                 2.2.1 Flow through packed beds
                 2.2.2 Minimum fluidisation conditions
                 2.2.3 Types of fluidisation
                 2.2.4 Fully fluidised beds
                 2.2.5 Bubbling
             2.3 Particle residence time
                 2.3.1 Mean residence time
                 2.3.2 Residence time distribution in well-mixed beds
                 2.3.3 Residence time distribution in plug flow beds
                 2.3.4 Multi-stage beds
                 2.3.5 Deviations in residence time distribution
             2.4 Gas residence time
                 2.4.1 Mean residence time
                 2.4.2 Bubbling fluidised beds
             2.5 Distributor design
             2.6 Elutriation and entrainment
             2.7 Attrition
             2.8 Physical forces
         3. HEAT TRANSFER
             3.1 Introduction
             3.2 Gas-to-particle heat transfer
             3.3. Heat transfer to walls
             3.4 Heat transfer from surfaces
             3.5 Heat transfer between particles
             3.6 Heat balance on a single particle
             3.7 Gas temperature profile within the bed
             3.8 Fluidised bed coolers
         4. MASS TRANSFER AND DRYING KINETICS
             4.1 Description of mass transfer processes
             4.2 Equilibrium moisture content
             4.3 Theoretical models for internal moisture transport
             4.4 Vapour diffusion
             4.5 The characteristic drying curve
             4.6 Experimental measurements of drying rates
             4.7 Overall models for fluidised bed dryers
             4.8 Normalisation of batch drying curves
                 4.8.1 Batch and plug-flow continuous beds
                 4.8.2 Well-mixed continuous beds
                 4.8.3 Elevated humidities
                 4.8.4 Applicability of normalisation rules
                 4.8.5 Saturation
             4.9 Drying in fluidised bed coolers
         5. MODELS AND DESIGN PROCEDURES
             5.1 Open literature review
             5.2 Overall heat and mass balance
             5.3 Scale-up methods
             5.4 SPS design procedures
             5.5 Economic factors in design
                 5.5.1 Capital cost
                 5.5.2 Operating costs
                 5.5.3 Effect of design conditions on costs
         6. CONCLUSIONS AND RECOMMENDATIONS
             6.1 State of current knowledge
             6.2 Recommendations for future work
         7 REFERENCES
         8 NOMENCLATURE
             8.1 Subscripts
             8.2 Greek
     Part 4: Design Guide
         1 INTRODUCTION
         2 FORMULATION OF THE DESIGN PROBLEM
         3 SCOPING DESIGN CALCULATIONS
             3.1 Introduction
             3.2 Design mode
                 3.2.1 Worked example
             3.3 Performance mode
                 3.3.1 Worked example
         4 PRELIMINARY PROCESS AND EQUIPMENT SELECTION
         5 OBTAINING DESIGN DATA
             5.1 Introduction
             5.2 Generation of batch drying data
                 5.2.1 Introduction
                 5.2.2 Measurement of batch drying curves
                 5.2.3 Verification of normalisation rules
                 5.2.4 Limiting factor for the drying rate
                 5.2.5 Worked example
             5.3 Measurement of drying equilibria
                 5.3.1 Experimental methods
                 5.3.2 Formulae for equilibrium moisture content
                 5.3.3 Worked example
             5.4 Generation of fluidisation data
                 5.4.1 Introduction
                 5.4.2 Measurements with room temperature air
                 5.4.3 Theoretical prediction of fluidisation velocities
                 5.4.4 Estimating fluidisation data at process conditions
                 5.4.5 Worked example 1 - theoretical prediction of fluidisation velocities
                 5.4.6 Worked example 2 - scale-up of experimental fluidisation velocities
         6 FULL-SCALE DESIGN PROCEDURE
             6.1 Layout of calculation procedure
             6.2 Initial selection of full-scale design conditions
                 6.2.1 Worked example
             6.3 Calculation of design curves and completion of design
             6.4 Well-mixed fluidised bed dryers
                 6.4.1 Worked example - indirectly heated dryer
                 6.4.2 Worked example - direct-fired dryer
                 6.4.3 Worked example - dryer with exhaust gas recycle
                 6.4.4 Worked example - internal heating coils
             6.5 Plug-flow fluidised bed dryers
                 6.5.1 Rotating rake at feed end
                 6.5.2 Worked example - indirectly heated dryer
                 6.5.3 Worked example - exhaust gas recycle
                 6.5.4 Worked example - partial Type B normalisation
                 6.5.5 Worked example - internal heating coils
             6.6 Multi-stage fluidised bed dryers
                 6.6.1 Introduction
                 6.6.2 n equal-sized well-mixed stages in series
                 6.6.3 Single well-mixed stage + single plug-flow stage
             6.7 Batch fluidised bed dryers
                 6.7.1 Worked example
             6.8 Vibro-fluidised bed dryers
             6.9 Comparisons and conclusions
         7 PILOT PLANT TESTS
             7.1 Introduction
             7.2 Experimental method
             7.3 Reasons for discrepancies between predicted and measured performance
             7.4 Correcting the design curve using pilot-plant data
                 7.4.1 Worked example
         8 ANCILLARY AND SUPPORTING CALCULATIONS
             8.1 Introduction
             8.2 Physical property calculations
                 8.2.1 Enthalpy and heat capacity
                 8.2.2 Saturation vapour pressure and temperature
                 8.2.3 Acid dew point
             8.3 Saturation of exhaust gas
             8.4 Calculations with gas recycle
                 8.4.1 Condenser conditions
                 8.4.2 Recycle ratio
                 8.4.3 Mass balance on dry gas
                 8.4.4 Mass balance on solvent
                 8.4.5 Heat balance
                 8.4.6 Worked example
             8.5 Heater duty
             8.6 Combustion calculations for direct-fired heater
                 8.6.1 Worked example
             8.7 Immersed heating coils
             8.8 Fan duty
             8.9 Distributor design
                 8.9.1 Worked example
             8.10 Plenum chamber design
             8.11 Freeboard design
             8.12 Elutriation and entrainment calculations
             8.13 Condenser design
             8.14 Insulation
         9 CONCLUSIONS
         10 REFERENCES
         11 NOMENCLATURE
     Part 5: Fluidised Bed Granulation and Coating
         1. INTRODUCTION
             1.1 Aims of the Report
             1.2 Summary of the Contents
             1.3 The basis of the Report
         2. THE TECHNOLOGICAL OPTIONS
             2.1 Introduction
             2.2 Fluidised Bed Granulators Versus Other Granulators
             2.3 Fluidised Bed Granulators Versus Crystallisers
             2.4 Fluidised Bed Granulators Versus Spray Dryers
                 2.4.1 Residence time distribution and mean residence time
                 2.4.2 Operating voidage
                 2.4.3 Thermal considerations
                 2.4.4 Particle morphology, strength, density and size distribution
             2.5 Combined Spray Dryer/Fluidised Bed Granulator/Fluidised Bed Dryers
             2.6 Fluidised Bed Granulators as Chemical Reactors
             2.7 Fluidised Bed Granulators versus Spouted Bed Granulators
             2.8 The Fluidised Bed as a Coater
             2.9 Batch Versus Continuous Fluidised Bed Granulation
         3. APPLICATIONS
             3.1 Granulation and "Crystallisation" Modes of Operating
             3.2 Coating
         4. PROCESS DESIGN AND EVALUATION: COATING, LAYERED AND AGGLOMERATE GROWTH
             4.1 Introduction
             4.2 Quantitative Aspects
                 4.2.1 Mass, Humidity and Heat Considerations
                 4.2.2 Fluidisation and Drying Characteristics
             4.3 Granulation Parameters and Granule Properties
                 4.3.1 Introduction
                 4.3.2 Coating
                 4.3.3 Layered Growth
                 4.3.4 Agglomerate Growth
             4.4 A Simple Test for Types of Growth
         5 LIQUID FEEDING METHODS
             5.1 Introduction
             5.2 The Choice of Atomizer Position and the Control of Droplet Size
         6. SOLIDS MANAGEMENT
             6.1 Solids Feeding
             6.2 Solids Mixing in a Fluidised Bed
             6.3 Solids Withdrawal
             6.4 Fines Recovery and Return
             6.5 Residence Time Distribution
             6.6 Particle Size Control
                 6.6.1 Batch Processes
                 6.6.2 Continuous Granulation and the Population Balance
                 6.6.3 A Simple Test of the Extent of Fines Recycling Required
         7. INSTRUMENTATION AND CONTROL
             7.1 The Simple Batch Granulator
             7.2 Detection and Control of Wet and Dry Quenching
             7.3 Control of Continuous Fluidised Bed Granulation
         8. SAFETY AND ENVIRONMENTAL CONSIDERATIONS
             8.1 Explosions
             8.2 Environmental Considerations
                 8.2.1 Air pollution control
                 8.2.2 Dust free discharge
         9. COST AND ECONOMIC FACTORS
             9.1 Introduction
             9.2 Costs of Batch Granulators
             9.3 Some Operating Cost Data for Continuous Operation
         10. FLUIDISATION PRINCIPLES
             10.1 Characterisation of Gas Fluidised Systems
             10.2 Minimum Fluidisation, Minimum Bubbling and Terminal Velocity
             10.3 Solids Mixing and Segregation
                 10.3.1 Monocomponent systems
                 10.3.2 Beds of Wide Size Distribution (Nienow and Chiba, 1985)
             10.4 Distributor Selection
         11. PARTICLE GROWTH AND REDUCTION MECHANISMS
             11.1 A Generalised Picture
             11.2 Effect of Process Parameters on General Description
                 11.2.1 Droplet Size
                 11.2.2 Bed Moisture Content
                 11.2.3 Attrition
                 11.2.4 Binder (Solution) Concentration
                 11.2.5 Type of binder
                 11.2.6 Wettability
                 11.2.7 Material to be Granulated
         12. MATHEMATICAL MODELS OF FLUIDISED BED GRANULATION
             12.1 Batch Systems
                 12.1.1 Layered Growth
                 12.1.2 Growth by Agglomeration
             12.2 Population Balance Models
         13. SMALL SCALE TESTS AND SCALE-UP
             13.1 Introduction
             13.2 A Decision Tree for Assesing and Optimising Granulation
             13.3 Binder Selection
             13.4 Scale-up Considerations
         14 SUMMARY OF THE PRESENT POSITION
         15. RECOMMENDATIONS FOR FURTHER WORK
             15.1 Instrumentation and Control
             15.2 Coating Processes
             15.3 Fine Particle Agglomeration
             15.4 Binder Selection
             15.5 Expert Systems
             15.6 Large Scale Test Facility
         16 NOMENCLATURE
             16.1 Greek Letters
             16.2 Subscripts and Superscripts
         17 REFERENCES
     Part 6: Vibro-fluidised Bed Dryers
         1. INTRODUCTION
         2. TECHNOLOGICAL OPTIONS
             2.1 Introduction
             2.2 Vibrofluidised bed dryers
                 2.2.1 Common Features
             2.3 Continuous units
                 2.3.1 Two-Mass Dryers
                 2.3.2 Single-Mass Dryer with Inclined Deck and Normal Vibrations
                 2.3.3 Single-Mass Dryer with Horizontal Deck and Angled Vibrations
             2.4 Batch units
             2.5 Vibrated through-circulation dryers
             2.6 Vibrated contact dryers
             2.7 Selection of gas velocity and bed depth
             2.8 Conclusions
         3. SAFETY AND OPERATIONAL FEATURES
             3.1 Introduction
             3.2 Fire and explosion hazards
                 3.2.1 Hazards Associated with Vibrated-Bed Drying
             3.3 Energy utilisation
                 3.3.1 Optimization of Operating Conditions
             3.4 Environmental considerations
             3.5 Maintenance
             3.6 Control
             3.7 Conclusions
         4. APPLICATIONS
             4.1 Introduction
             4.2 Selection criteria
             4.3 Industrial applications
             4.4 Conclusions
         5. THE FLUID-PARTICLE MECHANICS OF VIBRATED BEDS
             5.1 Introduction
             5.2 Fluidisation curves
             5.3 Velocity of incipient vibrofluidisation
             5.4 Pressure drop
             5.5 Bed voidage
             5.6 Solids mixing
             5.7 Conclusions
         6. THE MOTION OF SOLID PARTICLES ON VIBRATED SURFACES
             6.1 Introduction
             6.2 Vertical motion of the vibrated bed
             6.3 Bed motion along the length of the dryer
             6.4 Conclusions
         7. HEAT AND MASS TRANSFER IN VIBRATED BEDS
             7.1 Introduction
             7.2 Heat transfer by convection
             7.3 Mass transfer
             7.4 Conclusions
         8. DRYING IN VIBRATED BEDS
             8.1 Literature Survey
             8.2 Conclusions
         9. PROCESS DESIGN
             9.1 Introduction
             9.2 Design Procedure
                 9.2.1 Problem Definition
                 9.2.2 Tests on the Material
                 9.2.3 Dimensioning of the Dryer
                 9.2.4 Detailed Design of the Dryer
                 9.2.5 Mass and Heat Balances
                 9.2.6 Gas Cleaning Equipment
                 9.2.7 Power Requirements
                 9.2.8 Costing
             9.3 Conclusions
         10. CONCLUSIONS AND RECOMMENDATIONS
             10.1 Conclusions
             10.2 Recommendations
         11 REFERENCES
         12 NOMENCLATURE
             12.1 Subscripts
             12.2 Superscripts
             12.3 Greek
     Terms and Conditions of Use

Volume DRY III Part 1 Introduction.

This describes the basic features of fluidised bed dryers and their advantages and disadvantages relative to other types of dryer. It also explains how the volume is laid out and how to use it to best effect.


Volume DRY III Part 2 State of the technology.

This describes and illustrates current industrial fluidised bed dryers, and covers the main equipment options. Fluidised bed dryers can be categorised into well-mixed, plug-flow and multi-stage continuous units and batch units.

A well-mixed fluid bed dryer is usually of circular cross-section, and takes its name from the fact that the particle residence time distribution approaches the exponential perfect mixing law. Because of this, material in the bed has a nearly uniform temperature and a composition equal to that of the product stream. The wet feed thus falls into a bed of almost dry particles. Consequently, this type of fluid bed can handle wetter feedstocks than other types. In addition, its thermal efficiency can be comparatively high as the hot gas is utilised uniformly over the entire bed area. However, the product moisture content distribution can be quite broad.

In many applications either a narrow distribution of product moisture contents is required or the residence time of all the material must be reasonably uniform to guard against thermal degradation. "Plug flow" fluid bed dryers attempt to achieve a close approach to uniformity of particle residence time by having a high length-to-width ratio of the bed. The bed is usually shallow with an adjustable outlet weir. Disadvantages include difficulty in fluidising certain wet feeds, possible saturation of the exhaust gas near the inlet, and potential overheating of dry solids near the outlet. Multi-stage dryers may be used to reduce these problems. The drying behaviour in batch dryers is similar to that in plug-flow units and a uniform product is again achieved.

This Part also describes equipment and operational practice in the following areas: feeding, discharge, coolers, submerged heating surfaces, applications, operating problems, fire and explosion hazards, energy utilisation, maintenance and control.


Volume DRY III Part 3 State of the science.

This covers the underlying science of fluidised bed drying in depth, with the following main headings:

  • Fluidisation: gas flow, solids mixing patterns and residence time distributions, distributor effects, elutriation, entrainment and attrition.
  • Heat transfer: between hot gas, particles, walls and submerged heating surfaces.
  • Drying kinetics: mass transfer, batch drying curves, normalisation and scaling of drying curves to other conditions.
  • Design procedures: the theoretical basis of the SPS recommended procedures and the alternatives.

Volume DRY III Part 4 Design guide.

This part covers the design procedure for a new fluidised bed dryer or the performance assessment of an existing unit. The layout is designed to be compatible with the PC programs DRYCUR and FLUBED, which can be used to perform the calculations. Extensive worked examples are provided.

The design procedure is developed from the methods described in DR1 and DR3, now withdrawn. It uses data collected from a few simple batch drying tests and fluidisation measurements to predict the performance of a full-size unit under a wide variety of conditions. These calculations permit rapid preliminary equipment sizing and optimisation of operating conditions in advance of pilot plant testing.

The basic pattern of the design procedure is similar for all types of fluidised bed dryer. However, for well-mixed dryers the drying curve must be converted to isothermal bed conditions and further modified to allow for the range of residence times. Likewise, the plug-flow procedure includes an axial dispersion model which characterises the deviation from plug flow. The design procedure can be adapted to more complex cases, including vibro-fluidised bed dryers, beds fitted with internal heaters and beds with a rotating rake at the feed end.

The contents of the Part are as follows:

  • Formulation of the design problem, collection and collation of data
  • Preliminary process and equipment selection
  • Scoping design procedure (gives rough estimate of bed size)
  • Generation of fluidisation and drying data
  • Detailed design procedures for well-mixed, plug-flow, multi-stage and batch units
  • Pilot plant tests and scale-up

Ancillary design calculations: distributor, plenum chamber, freeboard, heater duty (indirect or direct-fired), gas recycle systems, fan and condenser.


Volume DRY III Part 5 Fluidised bed granulation and coating.

A fluidised bed can be utilised to produce hard, roughly spherical granules or loose agglomerates from solutions and slurries. It can also be used to apply a uniform coating of a second material over the particles. The report guides the reader through the technological options and applications to help him decide on the suitability of a fluidised bed, the most appropriate type of operation, the preliminary design of the plant and the solution of operating problems. Additional practical topics covered include instrumentation and control, feeding methods, solids classification and mixing, control of residence time distribution, costs, safety and environmental considerations. The considerable advances that have been made over the past few years in the fundamental science are critically reviewed. In particular, fluidisation, particle growth and reduction mechanisms are discussed. Published simulation models and the usefulness of small scale tests for evaluating feasibility and optimisation are assessed.


Volume DRY III Part 6 Vibro-fluidised bed dryers.

This part of Volume III covers the "State of the Technology" and "State of the Science" for vibro-fluidised bed dryers, as their behaviour is rather different to that of conventional fluidised beds.

In vibro-fluidised bed dryers, the bed of solids is fluidised and also subjected to sinusoidal vibrations. This technique is particularly useful for materials which are cohesive or pasty, have a wide size distribution, or are of low mechanical strength. The common and distinguishing features of the different units employed in industry are described. Typical applications are reviewed, together with the current practices relating to design and operation. The science of fluid-particle mechanics of vibrated-beds is discussed. Published theories and experimental studies of the effect of vibration on heat transfer and drying kinetics are compared and useful guidance on the probable effects of operating variables on dryer performance is compiled.